Sol-gel Preparation of Silan based Zirconia Hybrid Thin Film

نویسندگان

چکیده

The sol-gel process is an innovative advanced method, initially developed to synthesize glass and ceramics at low temperature. Sol-gel can be used synthesis materials with a variety of shapes, such as porous membranes, thin fibers, nano-size powders films. In this study, epoxy methacrylate based silane coupling agents are together zirconium oxide form hybrid coating system on surface. the experimental organic–inorganic molecular compound was prepared by method. First glasses were cleaned traditional piranha solution (3:1 H2SO4 : H2O2) remove contaminants. Silanization applied increase adhesion coatings substrates. Glass substrate coated homemade dip-coater. (3-Glycidoxypropyltrimethoxysilane, GLYMO 3-(trimethoxysilyl)propylmethacrylate, TMSPM) chosen silane. Zirconia inorganic component materails. Coated samples characterized Fouirer Transform Infrared Spectrophotometer (FTIR), Scanning Electron Microscope Energy Dispersive X-ray Spectroscopy (SEM-EDX) Contact Angle Goniometer.

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Article history: Development of non-volatil Received 13 September 2006 Received in revised form 10 February 2009 Accepted 12 February 2009 Available online 27 February 2009

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ژورنال

عنوان ژورنال: International journal of computational and experimental science and engineering

سال: 2021

ISSN: ['2149-9144']

DOI: https://doi.org/10.22399/ijcesen.727304